2-(2-chlorophenyl)-1-(piperidin-1-yl)ethaneselenone

Base Information

• Chemical Name: 2-(2-chlorophenyl)-1-(piperidin-1-yl)ethaneselenone
• CAS No.: 1427505-18-7
• Molecular Formula: C₁₃H₁₆ClNSe
• Molecular Weight: 300.69
• Mol file: 1427505-18-7.mol

Synonyms:2-(2-chlorophenyl)-1-(piperidin-1-yl)ethaneselenone

Chemical Property of 2-(2-chlorophenyl)-1-(piperidin-1-yl)ethaneselenone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-(2-chlorophenyl)-1-(piperidin-1-yl)ethaneselenone

There total 2 articles about 2-(2-chlorophenyl)-1-(piperidin-1-yl)ethaneselenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

piperidine (110-89-4) + 4-(2-chlorophenyl)-1,2,3-selenadiazole (1360685-01-3) → 2-(2-chlorophenyl)-1-(piperidin-1-yl)ethaneselenone (1427505-18-7)

Guidance literature:

With potassium hydroxide; at 55 ℃;

DOI:10.1021/ol400547n

Reference yield:

2'-chloroacetophenone semicarbazone → 2-(2-chlorophenyl)-1-(piperidin-1-yl)ethaneselenone (1427505-18-7)

Guidance literature:

Multi-step reaction with 2 steps

1: selenium(IV) oxide / acetic acid / 4 h / 65 °C

2: potassium hydroxide / 55 °C

With selenium(IV) oxide; potassium hydroxide; In acetic acid;

DOI:10.1021/ol400547n

upstream raw materials:

piperidine

4-(2-chlorophenyl)-1,2,3-selenadiazole