C₃₄H₃₆INO₆Si

Base Information

• Chemical Name: C₃₄H₃₆INO₆Si
• CAS No.: 1331965-91-3
• Molecular Formula: C₃₄H₃₆INO₆Si
• Molecular Weight: 709.653
• Mol file: 1331965-91-3.mol

Synonyms:C₃₄H₃₆INO₆Si

Chemical Property of C₃₄H₃₆INO₆Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₆INO₆Si

There total 9 articles about C₃₄H₃₆INO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-(2,3-bis(benzyloxy)phenyl)-6-iodobenzo[d][1,3]dioxole-5-carboxamide (1331965-87-7) + (2-trimethylethylsilylethoxy)methyl chloride (76513-69-4) → C34H36INO6Si (1331965-91-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1007/s12272-011-0703-1

Reference yield:

3,4-Bis(phenylmethoxy)benzeneamine (18002-44-3) → C34H36INO6Si (1331965-91-3)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

With sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;

DOI:10.1007/s12272-011-0703-1

Reference yield:

C23H23NO4 (79353-93-8) → C34H36INO6Si (1331965-91-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol / 18 h / Reflux; Inert atmosphere

2: triethylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

With sodium hydride; triethylamine; potassium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; mineral oil;

DOI:10.1007/s12272-011-0703-1

upstream raw materials:

3,4-dibenzyloxybenzaldehyde

6-iodobenzo[d][1,3]dioxole-5-carboxylic acid

C₂₃H₂₃NO₄

N-(2,3-bis(benzyloxy)phenyl)-6-iodobenzo[d][1,3]dioxole-5-carboxamide

Downstream raw materials:

2,3-bis(benzyloxy)-5-((2-(trimethylsilyl)ethoxy)methyl)-[1,3]dioxolo[4,5-j]phenanthridin-6(5H)-one

Refernces