p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate

Base Information

• Chemical Name: p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate
• CAS No.: 1005398-25-3
• Molecular Formula: C₁₂₁H₁₀₃N₂O₃₃S*F₆P
• Molecular Weight: 2290.17

Synonyms:p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate

Chemical Property of p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate

Chemical Property:

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Technology Process of p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate

There total 2 articles about p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

p-thiotolyl 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside (1005398-20-8) + [(6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl fluoride] hexafluorophosphate → p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate (1005398-25-3)

Guidance literature:

With bis(cyclopentadienyl)hafnium dichloride; silver perchlorate; In dichloromethane; at 0 ℃; Inert atmosphere; Molecular sieve;

DOI:10.1021/jo901169u

Reference yield: 81.0%

C33H30FN2O9(1+)*F6P(1-) (1005398-17-3) + p-tolyl 6-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside (1005398-23-1) → p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate (1005398-25-3)

Guidance literature:

With bis(cyclopentadienyl)hafnium dichloride; silver perchlorate; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ol702743x

Reference yield: 86.0%

p-tolyl (6-O-(1-methyl-3-imidazolio)acetyl)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-1-thio-2,3,4-tri-O-benzoyl-α-D-mannopyranoside hexafluorophosphate (1005398-25-3) → p-thiotolyl 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside (1005398-08-2)

Guidance literature:

With water; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; In diethyl ether; at 20 ℃;

DOI:10.1021/ol702743x

upstream raw materials:

C₃₃H₃₀FN₂O₉⁽¹⁺⁾*F₆P^(1-)

p-tolyl 6-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranosyl]-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

p-thiotolyl 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Downstream raw materials:

p-thiotolyl 2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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