6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one

Base Information

• Chemical Name: 6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one
• CAS No.: 1027210-26-9
• Molecular Formula: C₁₇H₁₅ClN₂O₂
• Molecular Weight: 314.771

Synonyms:6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one

Chemical Property of 6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one

Chemical Property:

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Technology Process of 6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one

There total 2 articles about 6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

β-p-Chlorbenzoyl-α-p-methoxyphenyl-propionsaeure-methylester (101733-24-8) → 6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one (1027210-26-9)

Guidance literature:

With hydrazine hydrate; In diethylene glycol; for 8h; Heating;

DOI:10.1081/SCC-100103250

Reference yield:

4-(4-chloro-phenyl)-2-(4-methoxy-phenyl)-4-oxo-butyronitrile (101602-36-2) → 6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one (1027210-26-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄ / Heating

2: 70 percent / N₂H₄*H₂O / bis-(2-hydroxy-ethyl) ether / 8 h / Heating

With sulfuric acid; hydrazine hydrate; In diethylene glycol;

DOI:10.1081/SCC-100103250

Reference yield: 79.0%

6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-4,5-dihydro-2H-pyridazin-3-one (1027210-26-9) → 6-(4-chloro-phenyl)-4-(4-methoxy-phenyl)-2H-pyridazin-3-one

Guidance literature:

With selenium(IV) oxide; for 0.0833333h; microwave irradiation;

DOI:10.1081/SCC-100103250

upstream raw materials:

β-p-Chlorbenzoyl-α-p-methoxyphenyl-propionsaeure-methylester

4-(4-chloro-phenyl)-2-(4-methoxy-phenyl)-4-oxo-butyronitrile

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