methyl -alaninate

Base Information

Chemical Name:methyl -alaninate
CAS No.:174466-55-8
Molecular Formula:C₁₁H₁₆N₂O₄S
Molecular Weight:272.325
Hs Code.:

methyl <N-(N'-benzyl)-sulfamoyl>-alaninate

Synonyms:methyl -alaninate

Suppliers and Price of methyl -alaninate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl -alaninate

Chemical Property:

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Technology Process of methyl -alaninate

There total 2 articles about methyl -alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 174466-51-4
<(S)(-)> methyl -alaninate

: 174466-55-8
methyl -alaninate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h;
DOI:10.1016/0040-4020(95)00932-9

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 174466-55-8
methyl -alaninate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / diethylazodicarboxylate, PPh₃ / tetrahydrofuran / 0.75 h / 5 °C

2: 92 percent / TFA / CH₂Cl₂ / 2 h

With triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4020(95)00932-9