6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

Base Information

Chemical Name:6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide
CAS No.:67287-63-2
Molecular Formula:BrH*C₁₆H₁₆ClNO₃
Molecular Weight:386.673
Hs Code.:

Synonyms:6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

Suppliers and Price of 6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

There total 5 articles about 6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 67287-60-9
N-[2-(2-chloro-3,4-dimethoxyphenyl)-ethyl]-2-hydroxy-2-(m-methoxyphenyl)ethylamine

: 67287-63-2
6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

Guidance literature:: With hydrogen bromide; at 135 ℃; for 3h;
DOI:10.1021/jm00346a005

Reference yield:

: 32017-77-9,53631-49-5
2-(m-methoxyphenyl)oxirane

: 67287-63-2
6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 18 h / 110 °C

2: 66 percent / 48percent aq. HBr / 3 h / 135 °C

With hydrogen bromide;
DOI:10.1021/jm00346a005

Reference yield:

: 67287-36-9
2-(2-chloro-3,4-dimethoxyphenyl)ethylamine

: 67287-63-2
6-chloro-7,8-dihydroxy-1-(m-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 18 h / 110 °C

2: 66 percent / 48percent aq. HBr / 3 h / 135 °C

With hydrogen bromide;
DOI:10.1021/jm00346a005