(S)-6-(1-Ethyl-propoxycarbonylmethyl)-cyclohex-1-enecarboxylic acid 1-ethyl-propyl ester

Base Information

Chemical Name:(S)-6-(1-Ethyl-propoxycarbonylmethyl)-cyclohex-1-enecarboxylic acid 1-ethyl-propyl ester
CAS No.:915295-93-1
Molecular Formula:C₁₉H₃₂O₄
Molecular Weight:324.461
Hs Code.:

Synonyms:(S)-6-(1-Ethyl-propoxycarbonylmethyl)-cyclohex-1-enecarboxylic acid 1-ethyl-propyl ester

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Chemical Property of (S)-6-(1-Ethyl-propoxycarbonylmethyl)-cyclohex-1-enecarboxylic acid 1-ethyl-propyl ester

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Technology Process of (S)-6-(1-Ethyl-propoxycarbonylmethyl)-cyclohex-1-enecarboxylic acid 1-ethyl-propyl ester

There total 2 articles about (S)-6-(1-Ethyl-propoxycarbonylmethyl)-cyclohex-1-enecarboxylic acid 1-ethyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 915295-88-4
(1S,2S,6S)-2-(1-Ethyl-propoxycarbonylmethyl)-6-[methyl-((S)-1-phenyl-ethyl)-amino]-cyclohexanecarboxylic acid 1-ethyl-propyl ester

: 915295-93-1
(S)-6-(1-Ethyl-propoxycarbonylmethyl)-cyclohex-1-enecarboxylic acid 1-ethyl-propyl ester

: (1S,2S,6S)-2-(1-Ethyl-propoxycarbonylmethyl)-6-(hydroxy-methyl-amino)-cyclohexanecarboxylic acid 1-ethyl-propyl ester

: N-Methyl-N-((S)-1-phenyl-ethyl)-hydroxylamine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; for 18h;
DOI:10.1016/j.tetasy.2006.06.048

Reference yield:

: dipent-3-yl (E,E)-nona-2,7-dienedioate

: 915295-93-1
(S)-6-(1-Ethyl-propoxycarbonylmethyl)-cyclohex-1-enecarboxylic acid 1-ethyl-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / tetrahydrofuran / -78 °C

2: 65 percent / m-chloroperbenzoic acid / 18 h

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; 2: Cope elimination;
DOI:10.1016/j.tetasy.2006.06.048