Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester
CAS No.:81188-33-2
Molecular Formula:C₁₉H₁₆O₆S
Molecular Weight:372.398
Hs Code.:

Synonyms:Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester

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Technology Process of Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester

There total 1 articles about Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 80596-50-5
2-hydroxymethyl-5-methoxy-1,4-naphthoquinone

: 81188-33-2
Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester

Guidance literature:: In pyridine; chloroform; at 50 ℃; for 2h;
DOI:10.1002/ardp.19813141214

Reference yield:

: 81188-33-2
Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester

: 481-42-5
5-hydroxy-2-methyl-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Zn powder, 2.) 30percent H₂O₂ / 1.) 80percent acetic acid, 12 h, room temp., 2.) 30 min

2: 90 percent / AlCl₃ / CH₂Cl₂ / 1.) 1 h, room temp., 2.) 15 min, water

With aluminium trichloride; dihydrogen peroxide; zinc; In dichloromethane;
DOI:10.1002/ardp.19813141214

Reference yield:

: 81188-33-2
Toluene-4-sulfonic acid 5-methoxy-1,4-dioxo-1,4-dihydro-naphthalen-2-ylmethyl ester

: 22266-99-5
2-methyl-5-methoxy-1,4-naphthoquinone

Guidance literature:: With dihydrogen peroxide; zinc; Yield given. Multistep reaction; 1.) 80percent acetic acid, 12 h, room temp., 2.) 30 min;
DOI:10.1002/ardp.19813141214