ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate

Base Information

Chemical Name:ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate
CAS No.:945722-00-9
Molecular Formula:C₂₆H₂₄FNO₆
Molecular Weight:465.478
Hs Code.:

Synonyms:ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate

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Chemical Property of ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate

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Technology Process of ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate

There total 4 articles about ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 73781-63-2
ethyl 2-(4-amino-2-fluoro-phenyl)acetate

: 1,4-bis(ethyloxy)-2,3-naphthalenedicarboxylic acid sodium salt

: 945722-00-9
ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate

Guidance literature:: With acetic acid; for 6h; Product distribution / selectivity; Heating / reflux;

Reference yield:

: 325780-76-5
1,4-bis(ethyloxy)-2,3-naphthalenedicarboxylic acid

: 73781-63-2
ethyl 2-(4-amino-2-fluoro-phenyl)acetate

: 945722-00-9
ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate

Guidance literature:: With acetic acid; for 28h; Product distribution / selectivity; Heating / reflux;

Reference yield:

: 84-66-2
Diethyl phthalate

: 945722-00-9
ethyl {4-[4,9-bis(ethyloxy)-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl]-2-fluorophenyl}acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / ethanol

2: sodium ethanolate / ethanol

3: acetic acid

With sodium ethanolate; acetic acid; In ethanol;
DOI:10.1016/j.bmcl.2018.03.091