6-methoxy-8-nitro-5--4-vinylquinoline

Base Information

Chemical Name:6-methoxy-8-nitro-5--4-vinylquinoline
CAS No.:98509-97-8
Molecular Formula:C₁₉H₁₃F₃N₂O₄
Molecular Weight:390.318
Hs Code.:

6-methoxy-8-nitro-5-<m-(trifluoromethyl)phenoxy>-4-vinylquinoline

Synonyms:6-methoxy-8-nitro-5--4-vinylquinoline

Suppliers and Price of 6-methoxy-8-nitro-5--4-vinylquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methoxy-8-nitro-5--4-vinylquinoline

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Technology Process of 6-methoxy-8-nitro-5--4-vinylquinoline

There total 2 articles about 6-methoxy-8-nitro-5--4-vinylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 98509-96-7
6-methoxy-8-nitro-5-quinoline-4-carboxaldehyde

: 19493-09-5
Methylenetriphenylphosphorane

: 98509-97-8
6-methoxy-8-nitro-5--4-vinylquinoline

Guidance literature:: In tetrahydrofuran; hexane; for 2h; Ambient temperature;
DOI:10.1021/jm00149a004

Reference yield:

: 82333-37-7
6-methoxy-4-methyl-8-nitro-5-<3-(trifluoromethyl)phenoxy>quinoline

: 98509-97-8
6-methoxy-8-nitro-5--4-vinylquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / acetic acid, selenium dioxide / dioxane; acetic anhydride / Heating

2: 72 percent / tetrahydrofuran; hexane / 2 h / Ambient temperature

With selenium(IV) oxide; acetic acid; In tetrahydrofuran; 1,4-dioxane; hexane; acetic anhydride;
DOI:10.1021/jm00149a004