N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide

Base Information

Chemical Name:N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide
CAS No.:298205-03-5
Molecular Formula:C₁₇H₁₉N₃OS
Molecular Weight:313.423
Hs Code.:

Synonyms:N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide

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Chemical Property of N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide

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Technology Process of N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide

There total 3 articles about N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 26562-24-3
3-bromo-2-methoxypropene

: 298204-73-6
N-[4-(methylthio)phenyl]-3-pyridinecarboxamide

: 298205-03-5
N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide

Guidance literature:: N-[4-(methylthio)phenyl]-3-pyridinecarboxamide; With sodium hexamethyldisilazane; In tetrahydrofuran; for 0.25h;

3-bromo-2-methoxypropene; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jm0000719

Reference yield:

: 100-54-9,121697-66-3,1232169-17-3,68271-95-4
pyridine-3-carbonitrile

: 298205-03-5
N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium bis(trimethylsilyl) amide / tetrahydrofuran / 4 h / 25 °C

1.2: 96 percent / tetrahydrofuran / 4 h

2.1: sodium bis(trimethylsilyl) amide / tetrahydrofuran / 0.25 h

2.2: 24 percent / tetrahydrofuran / 20 °C

With sodium hexamethyldisilazane; In tetrahydrofuran; 1.1: deprotonation / 1.2: Addition / 2.1: deprotonation / 2.2: Alkylation;
DOI:10.1021/jm0000719

Reference yield:

: 104-96-1
4-methylsulfanylaniline

: 298205-03-5
N-(2-methoxy-2-propenyl)-N-[4-(methylthio)phenyl]-3-pyridinecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium bis(trimethylsilyl) amide / tetrahydrofuran / 4 h / 25 °C

1.2: 96 percent / tetrahydrofuran / 4 h

2.1: sodium bis(trimethylsilyl) amide / tetrahydrofuran / 0.25 h

2.2: 24 percent / tetrahydrofuran / 20 °C

With sodium hexamethyldisilazane; In tetrahydrofuran; 1.1: deprotonation / 1.2: Addition / 2.1: deprotonation / 2.2: Alkylation;
DOI:10.1021/jm0000719