7,8,9,10,11-Pentaphenyl-9H-cycloheptaacenaphthalin

Base Information

• Chemical Name: 7,8,9,10,11-Pentaphenyl-9H-cyclohepta
• Molecular Formula: C₄₇H₃₂
• Molecular Weight: 596.771

Synonyms:7,8,9,10,11-Pentaphenyl-9H-cycloheptaacenaphthalin

Chemical Property of 7,8,9,10,11-Pentaphenyl-9H-cyclohepta

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

There total 3 articles about 7,8,9,10,11-Pentaphenyl-9H-cycloheptaacenaphthalin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7,8,9,10,11-Pentaphenyl-6bH-cycloheptaacenaphthalin (107964-44-3) → 7,8,9,10,11-Pentaphenyl-9H-cycloheptaacenaphthalin (107964-25-0)

Guidance literature:

at 200 ℃;

DOI:10.1021/ja00897a037

Reference yield:

7,8,9,10,11-Pentaphenyl-9H-cycloheptaacenaphthalin-kation → 7,8,9,10,11-Pentaphenyl-9H-cycloheptaacenaphthalin (107964-25-0)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄

2: 200 °C

With lithium aluminium tetrahydride;

DOI:10.1021/ja00897a037

Reference yield:

acecyclone (641-57-6) + 1,2,3-triphenylcyclopropene (16510-49-9) → 7,8,9,10,11-Pentaphenyl-9H-cycloheptaacenaphthalin (107964-25-0)

Guidance literature:

In xylene; Heating;

DOI:10.1021/ja00897a037

upstream raw materials:

7,8,9,10,11-Pentaphenyl-6bH-cycloheptaacenaphthalin

acecyclone

1,2,3-triphenylcyclopropene

Downstream raw materials:

3-Brom-7,8,9,10,11-pentaphenyl-9H-cycloheptaacenaphthalin

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