(5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone

Base Information

Chemical Name:(5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone
CAS No.:1207372-52-8
Molecular Formula:C₂₆H₄₆O₃Si
Molecular Weight:434.735
Hs Code.:

Synonyms:(5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone

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Chemical Property of (5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone

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Technology Process of (5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone

There total 1 articles about (5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1207372-71-1
C₂₈H₄₈O₄Si

: 1207372-52-8
(5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 72h;
DOI:10.1055/s-0029-1216990

Reference yield: 94.0%

: 1207372-52-8
(5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone

: 814-49-3
diethyl chlorophosphate

: 1207372-53-9
(8R,2E,6E)-8-(tert-butyldimethylsilyloxy)-8-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3,7-dimethylocta-2,6-dienyl diethyl phosphate

Guidance literature:: With pyridine; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1216990

Reference yield: 70.0%

: 1207372-52-8
(5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone

: 1207372-54-0
(2S,3R,6S)-2-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-3-isopropyl-6-methylcyclohexanone

Guidance literature:: (5R,6S)-6-[(1R,2E,6E)-1-(tert-butyldimethylsilyloxy)-8-hydroxy-2,6-dimethylocta-2,6-dienyl]-5-isopropyl-2-methylcyclohex-2-enone; With bismuth(III) chloride; In ethanol; at 0 ℃; for 0.0833333h;

With sodium tetrahydroborate; In ethanol; at 0 ℃; for 4.5h;
DOI:10.1055/s-0029-1216990