4,5-bis(decoxy)-1,2-benzoquinone

Base Information

Chemical Name:4,5-bis(decoxy)-1,2-benzoquinone
CAS No.:161807-09-6
Molecular Formula:C₂₆H₄₄O₄
Molecular Weight:420.633
Hs Code.:

Synonyms:4,5-bis(decoxy)-1,2-benzoquinone

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Chemical Property of 4,5-bis(decoxy)-1,2-benzoquinone

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Technology Process of 4,5-bis(decoxy)-1,2-benzoquinone

There total 4 articles about 4,5-bis(decoxy)-1,2-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 161807-03-0
3,4-Bis(decoxy)phenol

: 161807-09-6
4,5-bis(decoxy)-1,2-benzoquinone

Guidance literature:: With potassium dihydrogenphosphate; potassium nitrososulfonate; tetrabutyl-ammonium chloride; In tetrahydrofuran; water; for 2h;

Reference yield:

: 112-29-8
1-bromo dodecane

: 161807-09-6
4,5-bis(decoxy)-1,2-benzoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / K₂CO₃ / dimethylformamide / 16 h / 100 °C

2: 65 percent / 35percent H₂O₂, H₂SO₄ / CHCl₃; methanol / 5 h / Ambient temperature

3: 80 percent / tetrabutylammonium chloride, KH₂PO₄, potassium nitrosodisulfonate / H₂O; tetrahydrofuran / 2 h / Ambient temperature

With potassium dihydrogenphosphate; potassiuim nitrosodisulfonate; sulfuric acid; tetrabutyl-ammonium chloride; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00145a004

Reference yield:

: 118468-34-1
3,4-didecyloxybenzaldehyde

: 161807-09-6
4,5-bis(decoxy)-1,2-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 35percent H₂O₂, H₂SO₄ / CHCl₃; methanol / 5 h / Ambient temperature

2: 80 percent / tetrabutylammonium chloride, KH₂PO₄, potassium nitrosodisulfonate / H₂O; tetrahydrofuran / 2 h / Ambient temperature

With potassium dihydrogenphosphate; potassiuim nitrosodisulfonate; sulfuric acid; tetrabutyl-ammonium chloride; dihydrogen peroxide; In tetrahydrofuran; methanol; chloroform; water;
DOI:10.1021/ja00145a004