C₄₈H₄₅Cl₂N₅O₁₆

Base Information

• Chemical Name: C₄₈H₄₅Cl₂N₅O₁₆
• CAS No.: 164515-55-3
• Molecular Formula: C₄₈H₄₅Cl₂N₅O₁₆
• Molecular Weight: 1018.82
• Mol file: 164515-55-3.mol

Synonyms:C₄₈H₄₅Cl₂N₅O₁₆

Chemical Property of C₄₈H₄₅Cl₂N₅O₁₆

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of C₄₈H₄₅Cl₂N₅O₁₆

There total 4 articles about C₄₈H₄₅Cl₂N₅O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

C53H53Cl2N5O18 (164515-65-5) → C48H45Cl2N5O16 (164515-55-3)

Guidance literature:

With trifluoroacetic acid;

DOI:10.1021/jo9506746

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → C48H45Cl2N5O16 (164515-55-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 0.9 g / NaHCO₃ / dioxane; H₂O / 7 h / -5 °C

2: 50 percent / CF₃CO₂H

With sodium hydrogencarbonate; trifluoroacetic acid; In 1,4-dioxane; water;

DOI:10.1021/jo9506746

Reference yield:

C59H49Cl2N7O19 → C48H45Cl2N5O16 (164515-55-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) PhNCS, 2.) CF₃CO₂H / 1.) Py, H₂O, room temperature, 2.) room temperature

2: 0.9 g / NaHCO₃ / dioxane; H₂O / 7 h / -5 °C

3: 50 percent / CF₃CO₂H

With sodium hydrogencarbonate; phenyl isothiocyanate; trifluoroacetic acid; In 1,4-dioxane; water;

DOI:10.1021/jo9506746

upstream raw materials:

C₅₃H₅₃Cl₂N₅O₁₈

di-tert-butyl dicarbonate

C₄₃H₃₇Cl₂N₅O₁₄

Downstream raw materials:

C₅₆H₅₁Cl₂N₅O₁₈

Refernces