(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol

Base Information

Chemical Name:(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol
CAS No.:957774-17-3
Molecular Formula:C₅₇H₅₈O₇
Molecular Weight:855.083
Hs Code.:

Synonyms:(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol

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Chemical Property of (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol

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Technology Process of (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol

There total 3 articles about (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₉H₆₂O₈

: 957774-17-3
(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol

Guidance literature:: With hydrogenchloride; In di-isopropyl ether; water; isopropyl alcohol; at 80 ℃; for 2h;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 957774-17-3
(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C

1.2: 0.25 h / -78 °C

2.1: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 1 h / 0 °C

3.1: hydrogenchloride / di-isopropyl ether; water; isopropyl alcohol / 2 h / 80 °C

With hydrogenchloride; triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; di-isopropyl ether; water; isopropyl alcohol; acetonitrile;

Reference yield:

: C₅₉H₆₂O₉

: 957774-17-3
(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-[4-(2-hydroxyethyl)benzyl]-4-methylphenyl]-D-glucitol

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 1 h / 0 °C

2: hydrogenchloride / di-isopropyl ether; water; isopropyl alcohol / 2 h / 80 °C

With hydrogenchloride; triethylsilane; boron trifluoride diethyl etherate; In di-isopropyl ether; water; isopropyl alcohol; acetonitrile;