(6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate

Base Information

Chemical Name:(6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate
CAS No.:23234-27-7
Molecular Formula:C₂₄H₃₇N₃O₆
Molecular Weight:463.574
Hs Code.:

Synonyms:(6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate

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Chemical Property of (6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate

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Technology Process of (6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate

There total 13 articles about (6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-methyl 2-((S)-4-methyl-2-(2,2,2-trifluoroacetamido)pentanamido)-3-phenylpropanoate

: 126027-07-4
tert-butyl N-[(1S)-1-methyl-2-oxo-propyl]carbamate

: 23234-27-7
(6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.bmcl.2018.12.032

Reference yield:

: 119767-94-1
Boc-L-Ala-L-Leu-(Z)-ΔPhe-OMe

: 123975-73-5
Boc-L-Ala-L-Leu-D-Phe-OMe

: 23234-27-7
(6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 1140 Torr; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1246/cl.1989.459

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: 38155-18-9
L-leucyl-L-phenylalanine methyl ester

: 23234-27-7
(6S,9S,12S)-methyl 12-benzyl-9-isobutyl-2,2,6-trimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oate

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2006.04.031