bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine

Base Information

• Chemical Name: bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine
• CAS No.: 326820-75-1
• Molecular Formula: C₅₂H₇₆N₄O₈S₄
• Molecular Weight: 1013.46

Synonyms:bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine

Chemical Property of bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine

Chemical Property:

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Technology Process of bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine

There total 3 articles about bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N-(3-bromo-propyl)-N-ethyl-2,4,6-trimethyl-benzenesulfonamide (161452-14-8) + N,N'-bis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine (221636-81-3) → bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine (326820-75-1)

Guidance literature:

N,N'-bis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

N-(3-bromo-propyl)-N-ethyl-2,4,6-trimethyl-benzenesulfonamide; In N,N-dimethyl-formamide; at 70 ℃; for 12h; Further stages.;

DOI:10.1021/jm000277+

Reference yield:

2-mesitylenesulphonyl chloride (773-64-8) → bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine (326820-75-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 82 percent / aq. NaOH / CH₂Cl₂ / 20 °C

2.1: NaH / dimethylformamide / 0.33 h / 0 °C

2.2: 73 percent / dimethylformamide / 12 h / 70 °C

With sodium hydroxide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm000277+

Reference yield:

trans-1,4-cyclohexyldiamine (2615-25-0) → bis[3-(ethylamino)propyl]-N,N',N'',N'''-tetrakis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine (326820-75-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 82 percent / aq. NaOH / CH₂Cl₂ / 20 °C

2.1: NaH / dimethylformamide / 0.33 h / 0 °C

2.2: 73 percent / dimethylformamide / 12 h / 70 °C

With sodium hydroxide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm000277+

upstream raw materials:

N-(3-bromo-propyl)-N-ethyl-2,4,6-trimethyl-benzenesulfonamide

N,N'-bis(mesitylenesulfonyl)-trans-1,4-cyclohexanediamine

2-mesitylenesulphonyl chloride

trans-1,4-cyclohexyldiamine

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