O-[2-(5-methyl-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethyl] 4-chloro-3-nitrophenylthiocarbamate

Base Information

Chemical Name:O-[2-(5-methyl-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethyl] 4-chloro-3-nitrophenylthiocarbamate
CAS No.:1152595-34-0
Molecular Formula:C₁₈H₁₄ClN₃O₅S
Molecular Weight:419.845
Hs Code.:

Synonyms:O-[2-(5-methyl-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethyl] 4-chloro-3-nitrophenylthiocarbamate

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Chemical Property of O-[2-(5-methyl-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethyl] 4-chloro-3-nitrophenylthiocarbamate

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Technology Process of O-[2-(5-methyl-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethyl] 4-chloro-3-nitrophenylthiocarbamate

There total 1 articles about O-[2-(5-methyl-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethyl] 4-chloro-3-nitrophenylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 223733-35-5
2-(2-hydroxyethyl)-5-methyl-1H-isoindole-1,3(2H)-dione

: 127142-66-9
1-chloro-4-isothiocyanato-2-nitrobenzene

: 1152595-34-0
O-[2-(5-methyl-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)ethyl] 4-chloro-3-nitrophenylthiocarbamate

Guidance literature:: 2-(2-hydroxyethyl)-5-methyl-1H-isoindole-1,3(2H)-dione; 1-chloro-4-isothiocyanato-2-nitrobenzene; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 24h; Cooling with ice;

With water; ammonium chloride; In N,N-dimethyl-formamide; mineral oil; pH=8;
DOI:10.1016/j.ejmech.2008.09.024