N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester
CAS No.:1202249-76-0
Molecular Formula:C₂₉H₂₅FNO₄P
Molecular Weight:501.494
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester

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Chemical Property of N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester

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Technology Process of N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester

There total 1 articles about N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2304-94-1
3-(benzyloxycarbonylamino)propanoic acid

: 2-(diphenylphosphanyl)-4-fluorophenol

: 1202249-76-0
N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.200900692

Reference yield: 85.0%

: 20379-59-3
D-glucopyranosyl azide

: 1202249-76-0
N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester

: 1202249-81-7
N-(N-benzyloxycarbonyl-β-alanyl)-β-D-glucopyranosylamine

Guidance literature:: D-glucopyranosyl azide; N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 20 - 40 ℃; Inert atmosphere;

With water; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 40 ℃; for 2h;
DOI:10.1002/ejoc.200900692

Reference yield: 71.0%

: 35899-89-9
1-amido-1-deoxygalactopyranose

: 1202249-76-0
N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester

: C₁₇H₂₄N₂O₈

: 1202249-85-1
N-(N-benzyloxycarbonyl-β-alanyl)-β-D-galactopyranosylamine

Guidance literature:: 1-amido-1-deoxygalactopyranose; N-(benzyloxycarbonyl)-β-alanine 2-(diphenylphosphanyl)-4-fluorophenyl ester; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 20 - 40 ℃; Inert atmosphere;

With water; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 40 ℃; for 2h;
DOI:10.1002/ejoc.200900692