(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate

Base Information

Chemical Name:(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate
CAS No.:83026-93-1
Molecular Formula:C₂₂H₂₂N₄O₇
Molecular Weight:454.439
Hs Code.:

Synonyms:(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate

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Technology Process of (2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate

There total 10 articles about (2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5987-73-5
2',3',5'-O-triacetyl-6-chloroinosine

: 98-80-6
phenylboronic acid

: 83026-93-1
(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In toluene; for 12h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201703723

Reference yield: 77.0%

: 15981-63-2
2',3',5'-tri-O-acetylnebularine

: 98-80-6
phenylboronic acid

: 83026-93-1
(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate

Guidance literature:: With ammonium peroxydisulfate; silver nitrate; trifluoroacetic acid; In water; 1,2-dichloro-ethane; at 20 ℃; for 3h; under 760.051 Torr; Reagent/catalyst; Solvent; Temperature; regioselective reaction; Catalytic behavior;
DOI:10.1002/ejoc.201700406

Reference yield: 70.0%

: 15981-63-2
2',3',5'-tri-O-acetylnebularine

: 98-80-6
phenylboronic acid

: (2R,3R,4R,5R)-2-(acetoxymethyl)-5-(8-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate

: 83026-93-1
(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate

: 107037-26-3
(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(2-phenyl-9H-purin-9-yl)tetrahydrofuran-3,4-diyldiacetate

Guidance literature:: With ammonium peroxydisulfate; silver nitrate; trifluoroacetic acid; In water; 1,2-dichloro-ethane; at 20 ℃; for 3h; under 760.051 Torr; regioselective reaction;
DOI:10.1002/ejoc.201700406