benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate

Base Information

Chemical Name:benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate
CAS No.:1125842-09-2
Molecular Formula:C₂₂H₂₇N₃O₃S
Molecular Weight:413.541
Hs Code.:

Synonyms:benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate

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Chemical Property of benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate

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Technology Process of benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate

There total 5 articles about benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 25126-45-8
(S)-benzyl 6-( tert-butoxycarbonylamino)-1-oxo-1-(phenylamino)hexan-2-ylcarbamate

: 870-73-5
ethyl dithioacetate

: 1125842-09-2
benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate

Guidance literature:: (S)-benzyl 6-( tert-butoxycarbonylamino)-1-oxo-1-(phenylamino)hexan-2-ylcarbamate; With trifluoroacetic acid; In ethyl acetate; at 0 - 20 ℃; for 2h;

With sodium carbonate; In water; ethyl acetate; at 0 ℃;

ethyl dithioacetate; With sodium carbonate; In ethanol; water;
DOI:10.1016/j.bmc.2010.06.035

Reference yield: 85.0%

: 870-73-5
ethyl dithioacetate

: 790999-53-0
5-tert-butoxycarbonylamino-1-phenylcarbamoylpentylamine

: 1125842-09-2
benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate

Guidance literature:: With sodium carbonate; In ethanol; water; at 20 ℃;
DOI:10.1016/j.bmcl.2009.08.028

Reference yield:

: 1125879-55-1
N²-((benzyloxy)carbonyl)-N⁶-ethanethioyl-L-lysine

: 62-53-3
aniline

: 1125842-09-2
benzyl (S)-(6-ethanethioamido-1-oxo-1-(phenylamino)hexan-2-yl)carbamate

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/acsmedchemlett.9b00580