1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

Base Information

• Chemical Name: 1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane
• CAS No.: 1433998-72-1
• Molecular Formula: C₂₉H₂₅O₄P
• Molecular Weight: 468.489
• Mol file: 1433998-72-1.mol

Synonyms:1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

Chemical Property of 1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

There total 1 articles about 1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

o-Allylphenol (1745-81-9) + 4-Hydroxyacetophenone (99-93-4) + 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (35948-25-5) → 1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane (1433998-72-1)

Guidance literature:

With toluene-4-sulfonic acid; at 60 ℃; for 12h; Inert atmosphere;

DOI:10.1002/pola.26549

Reference yield: 80.0%

1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane (1433998-72-1) + 4-Fluoronitrobenzene (350-46-9,178603-76-4) → C41H31N2O8P (1433998-73-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl acetamide; at 110 ℃; for 12h;

DOI:10.1002/pola.26549

Reference yield:

1-(3-allyl-4-hydroxyphenyl)-1-(4-hydoxyphenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane (1433998-72-1) → C41H35N2O4P (1433998-74-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl acetamide / 12 h / 110 °C

2: hydrogenchloride; iron / water; ethanol / 3 h / Reflux

With hydrogenchloride; iron; potassium carbonate; In ethanol; N,N-dimethyl acetamide; water;

DOI:10.1002/pola.26549

upstream raw materials:

o-Allylphenol

4-Hydroxyacetophenone

9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide

Downstream raw materials:

C₄₁H₃₅N₂O₄P

C₄₁H₃₁N₂O₈P