3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione

Base Information

Chemical Name:3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione
CAS No.:74731-76-3
Molecular Formula:C₂₄H₂₆N₂O₈
Molecular Weight:470.479
Hs Code.:

Synonyms:3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione

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Chemical Property of 3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione

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Technology Process of 3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione

There total 5 articles about 3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 7646-46-0
2-nitro-3-benzyloxy-4-methylbenzoic acid N-hydroxysuccinimide ester

: 74731-77-4
3-amino-4,9-dimethyl-1,5-dioxa-2,6-cyclononadione

: 74731-76-3
3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione

Guidance literature:: In tetrahydrofuran; 1.) 20 deg C, 20 h; 2.) 37 deg C, 48 h;

Reference yield:

: 27447-93-4
t-butyl γ-hydroxyvalerate

: 74731-76-3
3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione

Guidance literature:: Multi-step reaction with 5 steps

1: dicyclohexylcarbodiimide

2: trifluoroacetic acid

3: acetic anhydride / benzene

4: H₂ / Pd

5: 49 percent / tetrahydrofuran / 1.) 20 deg C, 20 h; 2.) 37 deg C, 48 h

With hydrogen; acetic anhydride; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; trifluoroacetic acid; benzene;

Reference yield:

: 22816-10-0
((2R,3S)-2,6-Dimethyl-4,9-dioxo-[1,5]dioxonan-3-yl)-carbamic acid benzyl ester

: 74731-76-3
3'-(2-nitro-3-benzyloxy-4-methylbenzoylamido)-4',9'-dimethyl-1',5'-dioxa-2',6'-cyclononadione

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd

2: 49 percent / tetrahydrofuran / 1.) 20 deg C, 20 h; 2.) 37 deg C, 48 h

With hydrogen; palladium; In tetrahydrofuran;