C₄₉H₆₂O₁₀Si

Base Information

Chemical Name:C₄₉H₆₂O₁₀Si
CAS No.:1345718-78-6
Molecular Formula:C₄₉H₆₂O₁₀Si
Molecular Weight:839.111
Hs Code.:

C<sub>49</sub>H<sub>62</sub>O<sub>10</sub>Si

Synonyms:C₄₉H₆₂O₁₀Si

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Chemical Property of C₄₉H₆₂O₁₀Si

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Technology Process of C₄₉H₆₂O₁₀Si

There total 7 articles about C₄₉H₆₂O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1345718-76-4
C₁₉H₃₈O₈Si

: 1345718-74-2
C₃₀H₂₆O₃

: 1345718-78-6
C₄₉H₆₂O₁₀Si

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In acetonitrile; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c1ob06047c

Reference yield:

: 112-50-5
monoethyl ether of triethylene glycol

: 1345718-78-6
C₄₉H₆₂O₁₀Si

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 16 h / Reflux

2: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide / acetonitrile / 24 h / 20 °C / Inert atmosphere

With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In toluene; acetonitrile;
DOI:10.1039/c1ob06047c

Reference yield:

: 105946-82-5
4-bromo-4'-iodobiphenyl

: 1345718-78-6
C₄₉H₆₂O₁₀Si

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 48 h / 70 °C / Inert atmosphere

3: potassium carbonate / methanol; dichloromethane / 3.5 h

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere

5: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide / acetonitrile / 24 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Sonogashira coupling / 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1039/c1ob06047c