Technology Process of C28H40N2O3Si
There total 7 articles about C28H40N2O3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
ethanol;
at 70 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Dess-Martin periodane / dichloromethane / 18 h / 20 °C / Cooling with ice
2: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C
3: 1H-imidazole / N,N-dimethyl-formamide / 18 h
4: lithium borohydride / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice
6: hydrazine hydrate / ethanol / 2 h / 70 °C
With
1H-imidazole; sodium tetrahydroborate; lithium borohydride; di-isopropyl azodicarboxylate; Dess-Martin periodane; hydrazine hydrate; triphenylphosphine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C
2: 1H-imidazole / N,N-dimethyl-formamide / 18 h
3: lithium borohydride / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice
5: hydrazine hydrate / ethanol / 2 h / 70 °C
With
1H-imidazole; sodium tetrahydroborate; lithium borohydride; di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;