Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester

Base Information

• Chemical Name: Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester
• CAS No.: 423158-70-7
• Molecular Formula: C₂₃H₃₂F₃NO₄S
• Molecular Weight: 475.573

Synonyms:Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester

Chemical Property of Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester

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Technology Process of Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester

There total 3 articles about Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(-)-aminomenthol (55179-51-6) → Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester (423158-70-7)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 20 °C

2: K₂CO₃ / acetonitrile / Heating

With potassium carbonate; In dichloromethane; acetonitrile;

DOI:10.1055/s-2002-19756

Reference yield:

2-formylphenyl triflate (84761-77-3) → Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester (423158-70-7)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 20 °C

2: K₂CO₃ / acetonitrile / Heating

With potassium carbonate; In dichloromethane; acetonitrile;

DOI:10.1055/s-2002-19756

Reference yield:

prenyl bromide (870-63-3) + Trifluoro-methanesulfonic acid 2-((2S,4aS,7R,8aR)-4,4,7-trimethyl-octahydro-benzo[e][1,3]oxazin-2-yl)-phenyl ester (423158-65-0) → Trifluoro-methanesulfonic acid 2-[(2S,4aS,7R,8aR)-4,4,7-trimethyl-3-(3-methyl-but-2-enyl)-octahydro-benzo[e][1,3]oxazin-2-yl]-phenyl ester (423158-70-7)

Guidance literature:

With potassium carbonate; In acetonitrile; Heating;

DOI:10.1055/s-2002-19756

upstream raw materials:

prenyl bromide

Trifluoro-methanesulfonic acid 2-((2S,4aS,7R,8aR)-4,4,7-trimethyl-octahydro-benzo[e][1,3]oxazin-2-yl)-phenyl ester

(-)-aminomenthol

2-formylphenyl triflate

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