2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester

Base Information

Chemical Name:2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester
CAS No.:97049-77-9
Molecular Formula:C₁₁H₁₁NO₄
Molecular Weight:221.213
Hs Code.:

Synonyms:2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester

There total 2 articles about 2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 79017-08-6,97049-60-0,97049-75-7
3-(1-nitroethyl)-1(3H)-isobenzofuranone

: 77-78-1
dimethyl sulfate

: 97049-77-9
2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester

Guidance literature:: With potassium carbonate; In acetone; for 18h; Ambient temperature;
DOI:10.1139/v85-061

Reference yield:

: 79017-08-6,97049-60-0,97049-75-7
3-(1-nitroethyl)-1(3H)-isobenzofuranone

: 97049-77-9
2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester

Guidance literature:: With potassium carbonate; dimethyl sulfate; In acetone; benzene;

Reference yield:

: 97049-77-9
2-<(2-methyl-2-nitro)ethylene>benzoic acid methyl ester

: 79017-19-9,79017-45-1,79017-20-2
1α-methyl-1,2,3,4,6,10b-hexahydropyrazino<2,1-a>isoindole

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate / acetonitrile / 4 h

2: 0.880 g / H₂ / 10percent Pd/C / acetic acid; H₂O / 18 h / 2585.7 Torr / Ambient temperature

3: H₂ / 10percent Pd/C / methanol; aq. HCl / 48 h / 760 Torr / Ambient temperature

4: 1 M solution of diborane / tetrahydrofuran / 18 h / Heating

With hydrogen; sodium acetate; diborane; palladium on activated charcoal; In tetrahydrofuran; hydrogenchloride; methanol; water; acetic acid; acetonitrile;
DOI:10.1139/v85-061