methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate

Base Information

Chemical Name:methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate
CAS No.:1296689-51-4
Molecular Formula:C₂₄H₃₁NO₂
Molecular Weight:365.516
Hs Code.:

Synonyms:methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate

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Chemical Property of methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate

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Technology Process of methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate

There total 1 articles about methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 3886-70-2
(R)-1-(1-Naphthyl)ethylamine

: 85636-50-6
1-(trimethylsiloxy)-1-methoxy-1,3-butadiene

: 2043-61-0
cyclohexanecarbaldehyde

: methyl (R,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate

: 1296689-51-4
methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate

Guidance literature:: (R)-1-(1-Naphthyl)ethylamine; cyclohexanecarbaldehyde; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

1-(trimethylsiloxy)-1-methoxy-1,3-butadiene; With tin(II) trifluoromethanesulfonate; In dichloromethane; at -78 - -30 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tetlet.2011.01.090

Reference yield: 92.0%

: 1296689-51-4
methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate

: 1296689-53-6
(S)-6-cyclohexylpiperidin-2-one

Guidance literature:: With palladium on carbon; hydrogen; In ethyl acetate;
DOI:10.1016/j.tetlet.2011.01.090

Reference yield:

: 1296689-51-4
methyl (S,E)-5-((R)-1-(naphthalen-1-yl)ethylamino)-5-cyclohexylpent-2-enoate

: 1030321-79-9
C₁₁H₂₁N

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on carbon; hydrogen / ethyl acetate

2: lithium aluminium tetrahydride / tetrahydrofuran / 50 °C

With lithium aluminium tetrahydride; palladium on carbon; hydrogen; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.tetlet.2011.01.090