6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol

Base Information

Chemical Name:6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol
CAS No.:84078-65-9
Molecular Formula:C₁₈H₃₂O
Molecular Weight:264.451
Hs Code.:

Synonyms:6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol

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Chemical Property of 6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol

Chemical Property:

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Technology Process of 6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol

There total 13 articles about 6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 84078-64-8
3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-methylenebutyl>-3-methyloxetane

: 84078-65-9
6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol

Guidance literature:: With lithium; ethylenediamine; In diethyl ether; for 0.5h;
DOI:10.1039/P19830001783

Reference yield:

: 84078-59-1
2-(2'-Methylene-6',6'-dimethylcyclohexyl)ethanol

: 84078-65-9
6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / nBu₃P / CH₂Cl₂ / 0 °C

2: 83 percent / Me₃SiOOSiMe₃ / benzene / 18 h / Heating

3: 78 percent / BuLi / tetrahydrofuran / -78 - 20 °C

4: 1) BuLi, 2) Et₃N / 1) THF, -10 deg C, 2) CH₂Cl₂

5: 75 percent / Na(Hg) / tetrahydrofuran; methanol / 0 °C

6: 95 percent / Li-H₂NCH₂CH₂NH₂ / diethyl ether / 15 °C

With n-butyllithium; sodium amalgam; tributylphosphine; bis-trimethylsilanyl peroxide; lithium; ethylenediamine; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene;
DOI:10.1039/c39820001078

Reference yield:

: 84078-60-4
1-(2-phenylthioethyl)-2-methylene-6,6-dimethylcyclohexane

: 84078-65-9
6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / Me₃SiOOSiMe₃ / benzene / 18 h / Heating

2: 78 percent / BuLi / tetrahydrofuran / -78 - 20 °C

3: 1) BuLi, 2) Et₃N / 1) THF, -10 deg C, 2) CH₂Cl₂

4: 75 percent / Na(Hg) / tetrahydrofuran; methanol / 0 °C

5: 95 percent / Li-H₂NCH₂CH₂NH₂ / diethyl ether / 15 °C

With n-butyllithium; sodium amalgam; bis-trimethylsilanyl peroxide; lithium; ethylenediamine; triethylamine; In tetrahydrofuran; methanol; diethyl ether; benzene;
DOI:10.1039/c39820001078