1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol

Base Information

Chemical Name:1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol
CAS No.:1335001-28-9
Molecular Formula:C₂₀H₂₆O₇
Molecular Weight:378.422
Hs Code.:

Synonyms:1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol

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Chemical Property of 1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol

Chemical Property:

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Technology Process of 1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol

There total 1 articles about 1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 496955-33-0
2-[2-(methoxymethoxy)phenyl]acetaldehyde

: 87746-55-2
1,4-dimethoxy-2-(methoxymethoxy)benzene

: 1335001-28-9
1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol

Guidance literature:: 1,4-dimethoxy-2-(methoxymethoxy)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 40 ℃; for 2h; Inert atmosphere;

With cerium(III) chloride; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

2-[2-(methoxymethoxy)phenyl]acetaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201100845

Reference yield:

: 1335001-28-9
1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol

: 407-25-0
trifluoroacetic anhydride

: 1335001-31-4
C₂₂H₂₅F₃O₈

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1002/ejoc.201100845

Reference yield:

: 1335001-28-9
1-[3,6-dimethoxy-2-(methoxymethoxy)phenyl]-2-[2-(methoxymethoxy)phenyl]ethanol

: 1335001-29-0
1,4-dimethoxy-2-methoxymethoxy-3-[2-(methoxymethoxy)phenethyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 0.5 h / 0 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h / 20 °C

With dmap; palladium 10% on activated carbon; hydrogen; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1002/ejoc.201100845