N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine

Base Information

• Chemical Name: N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine
• CAS No.: 1409949-77-4
• Molecular Formula: C₁₉H₁₉N₂P
• Molecular Weight: 306.347
• Mol file: 1409949-77-4.mol

Synonyms:N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine

Chemical Property of N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine

Chemical Property:

Purity/Quality:

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Technology Process of N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine

There total 2 articles about N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

→ N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine (1409949-77-4)

Guidance literature:

Reference yield: 91.0%

2-pyrrole aldehyde (1003-29-8,254729-95-8) + (2-aminoethyl)diphenylphosphane (4848-43-5) → N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine (1409949-77-4)

Guidance literature:

In ethanol; at 20 ℃; for 3h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jinorgbio.2020.111015

Reference yield: 85.0%

cis-dibromo-(cyclooctadiene)palladium(II) (12145-47-0) + N-((1H-pyrrol-2-yl)methylene)-2-(diphenylphosphino)ethanamine (1409949-77-4) → C19H18BrN2PPd

Guidance literature:

With triethylamine; In ethanol; dichloromethane; at 80 ℃; for 3h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jinorgbio.2020.111015

upstream raw materials:

2-pyrrole aldehyde

(2-aminoethyl)diphenylphosphane