2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose

Base Information

• Chemical Name: 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose
• CAS No.: 1256394-00-9
• Molecular Formula: C₅₄H₄₈O₁₄
• Molecular Weight: 920.967

Synonyms:2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose

Chemical Property of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose

Chemical Property:

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Technology Process of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose

There total 3 articles about 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

phenyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside (62774-33-8) + 1,6-Anhydro-2,3-di-O-benzyl-β-D-glucopyranose (80325-47-9) → 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose (1256394-00-9)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; (((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane); In dichloromethane; at -40 - 20 ℃; for 2.5h; Inert atmosphere; Molecular sieve;

DOI:10.1021/ol501211z

Reference yield: 72.0%

C73H70O15Si (1256394-06-5) → 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose (1256394-00-9)

Guidance literature:

With gold(III) tribromide; In acetonitrile; at 70 ℃; for 20h; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.09.004

Reference yield: 68.0%

C71H70O15Si (1256394-07-6) → 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-1,6-anhydro-2,3-di-O-benzyl-β-D-glucopyranose (1256394-00-9)

Guidance literature:

With gold(III) tribromide; In acetonitrile; at 70 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.09.004

upstream raw materials:

C₇₃H₇₀O₁₅Si

C₇₁H₇₀O₁₅Si

phenyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

1,6-Anhydro-2,3-di-O-benzyl-β-D-glucopyranose

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