C₂₂H₂₈F₃NO₇

Base Information

Chemical Name:C₂₂H₂₈F₃NO₇
CAS No.:1428245-72-0
Molecular Formula:C₂₂H₂₈F₃NO₇
Molecular Weight:475.462
Hs Code.:

C<sub>22</sub>H<sub>28</sub>F<sub>3</sub>NO<sub>7</sub>

Synonyms:C₂₂H₂₈F₃NO₇

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Chemical Property of C₂₂H₂₈F₃NO₇

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Technology Process of C₂₂H₂₈F₃NO₇

There total 11 articles about C₂₂H₂₈F₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1428245-84-4
(1S,2R,3S)-3-(1,3-dioxan-2-yl)-3-methyl-2-(nitromethyl)cyclohexanol

: 17257-71-5,20445-31-2,56135-03-6,81655-41-6
(S)-Mosher acid

: 1428245-72-0
C₂₂H₂₈F₃NO₇

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2013.02.078

Reference yield:

: 6-((tert-butyldimethylsilyl)oxy)-2-methylhexanal

: 1428245-72-0
C₂₂H₂₈F₃NO₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 0 °C

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 2 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 °C / Inert atmosphere

3.1: ammonium chloride / tetrahydrofuran / -78 - 30 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C

4.2: 12 h / 20 °C

5.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide; sodium periodate / diethyl ether; water / 24 h / 20 °C

6.1: triethylamine / 15 h / 20 °C

6.2: 2 h / -78 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane; water / 18 h / 0 - 20 °C

8.1: L-proline / methanol / 25 °C

9.1: pyridinium p-toluenesulfonate / toluene / Reflux

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 2 h / 0 - 20 °C

11.1: diisopropyl-carbodiimide; dmap / dichloromethane / 24 h / 20 °C

With dmap; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; sodium hydride; ammonium chloride; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; L-proline; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; 2.2: |Swern Oxidation / 6.2: |Henry Nitro Aldol Condensation / 8.1: |Michael Addition;
DOI:10.1016/j.tet.2013.02.078

Reference yield:

: 7-(1,3-dioxan-2-yl)oct-1-en-3-ol

: 1428245-72-0
C₂₂H₂₈F₃NO₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C

1.2: 12 h / 20 °C

2.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide; sodium periodate / diethyl ether; water / 24 h / 20 °C

3.1: triethylamine / 15 h / 20 °C

3.2: 2 h / -78 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane; water / 18 h / 0 - 20 °C

5.1: L-proline / methanol / 25 °C

6.1: pyridinium p-toluenesulfonate / toluene / Reflux

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 2 h / 0 - 20 °C

8.1: diisopropyl-carbodiimide; dmap / dichloromethane / 24 h / 20 °C

With dmap; sodium periodate; osmium(VIII) oxide; pyridinium p-toluenesulfonate; sodium hydride; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; L-proline; diisopropyl-carbodiimide; In methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; 3.2: |Henry Nitro Aldol Condensation / 5.1: |Michael Addition;
DOI:10.1016/j.tet.2013.02.078