C₄₇H₄₉FN₆O₅

Base Information

Chemical Name:C₄₇H₄₉FN₆O₅
CAS No.:639492-27-6
Molecular Formula:C₄₇H₄₉FN₆O₅
Molecular Weight:796.942
Hs Code.:

C<sub>47</sub>H<sub>49</sub>FN<sub>6</sub>O<sub>5</sub>

Synonyms:C₄₇H₄₉FN₆O₅

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Chemical Property of C₄₇H₄₉FN₆O₅

Chemical Property:

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Technology Process of C₄₇H₄₉FN₆O₅

There total 8 articles about C₄₇H₄₉FN₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 639491-88-6
C₄₇H₄₉FN₆O₅

: 639492-27-6
C₄₇H₄₉FN₆O₅

Guidance literature:: With silica gel; In acetonitrile; at 180 ℃; for 0.666667h; microwave;
DOI:10.1016/j.tet.2003.04.008

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 639492-27-6
C₄₇H₄₉FN₆O₅

Guidance literature:: Multi-step reaction with 9 steps

1: 60 percent / Cs₂CO₃ / dimethylformamide / 115 °C

2: tetrahydrofuran / 0.75 h / -70 - 20 °C

3: 46.0 g / p-dimethylaminopyridine / CH₂Cl₂ / 3.5 h / 20 °C

4: 77 percent / HF; pyridine / 4 h / 20 °C

5: 74 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 3 h / 4 - 20 °C

6: K₂CO₃ / dimethylformamide / 5 h / 20 °C

7: dimethylformamide / 17 h / 20 °C

8: 77 percent / C39H32OP2 bis-phosphine; [(η³-allyl)PdCl]2 / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

9: 74 percent / silica gel / acetonitrile / 0.67 h / 180 °C / microwave

With pyridine; dmap; bis(η3-allyl-μ-chloropalladium(II)); C₃₉H₃₂OP₂ bis-phosphine; hydrogen fluoride; silica gel; potassium carbonate; caesium carbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 9: Claisen rearrangement;
DOI:10.1016/j.tet.2003.04.008

Reference yield:

: 692729-77-4
3-[4-(tert-butyl-dimethyl-silanyloxy)-butoxy]-benzaldehyde

: 639492-27-6
C₄₇H₄₉FN₆O₅

Guidance literature:: Multi-step reaction with 8 steps

1: tetrahydrofuran / 0.75 h / -70 - 20 °C

2: 46.0 g / p-dimethylaminopyridine / CH₂Cl₂ / 3.5 h / 20 °C

3: 77 percent / HF; pyridine / 4 h / 20 °C

4: 74 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 3 h / 4 - 20 °C

5: K₂CO₃ / dimethylformamide / 5 h / 20 °C

6: dimethylformamide / 17 h / 20 °C

7: 77 percent / C39H32OP2 bis-phosphine; [(η³-allyl)PdCl]2 / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

8: 74 percent / silica gel / acetonitrile / 0.67 h / 180 °C / microwave

With pyridine; dmap; bis(η3-allyl-μ-chloropalladium(II)); C₃₉H₃₂OP₂ bis-phosphine; hydrogen fluoride; silica gel; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 8: Claisen rearrangement;
DOI:10.1016/j.tet.2003.04.008