Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Base Information

• Chemical Name: Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4
• CAS No.: 130327-30-9
• Molecular Formula: C₂₄H₂₀B*C₂₇H₃₆Cl₂N₃OPRe
• Molecular Weight: 1025.92

Synonyms:Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Chemical Property of Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Chemical Property:

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Technology Process of Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

There total 1 articles about Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(C₆H₅)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

ReOCl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={ReOCl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-27-4) → Re(OP(C6H5)3)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OP(C6H5)3)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-30-9)

Guidance literature:

With triphenylphosphine; In dichloromethane; Schlenk or vacuum-line techniques, N2-glovebox, ambient temp.; addn. of CH2Cl2 to phosphine and Re-complex, stirred (1 d); concn. (50 %), filtration (from brown solids), evapn. (to 2-3 ml), addn. of Et2O, pptn., filtration, washed (Et2O), evapn.; elem. anal.;

Reference yield: 79.0%

Re(OP(C6H5)3)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OP(C6H5)3)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-30-9) → Re(OC(CH3)2)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OC(CH3)2)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-36-5)

Guidance literature:

With acetone; In acetone; byproducts: OP(C6H5)3; Schlenk or vacuum-line techniques, N2-glovebox, ambient temp.; addn. of acetone to Re-complex, soln. stirred (3 d); concn. (to 5 ml), addn. of Et2O, pptn., filtration, washed (Et2O), evapn.;

Reference yield:

Re(OP(C6H5)3)Cl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={Re(OP(C6H5)3)Cl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-30-9) → ReOCl2((CH3)NCH2CH2)3(1+)*B(C6H5)4(1-)={ReOCl2((CH3)NCH2CH2)3}B(C6H5)4 (130327-27-4)

Guidance literature:

With dimethyl sulfoxide; In dimethyl sulfoxide; byproducts: OP(C6H5)3, (CH3)2S; Schlenk or vacuum-line techniques, N2-glovebox, ambient temp.;

upstream raw materials:

ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Downstream raw materials:

Re(OP(CH₃)3)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(OP(CH₃)3)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Re(CH₃CN)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(CH₃CN)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

Re(C₅H₅N)Cl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={Re(C₅H₅N)Cl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

ReOCl₂((CH₃)NCH₂CH₂)3⁽¹⁺⁾*B(C₆H₅)4^(1-)={ReOCl₂((CH₃)NCH₂CH₂)3}B(C₆H₅)4

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