Technology Process of C24H16BNO2S
There total 5 articles about C24H16BNO2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C24H14BrNS;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 1h;
With
Triisopropyl borate;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethyl phosphite / 1,2-dichloro-benzene / 5 h / 150 °C
2.1: copper(l) iodide; potassium phosphate; ethylenediamine / toluene / 15 h / Reflux
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
3.2: 5 h / -78 - 20 °C
With
potassium phosphate; copper(l) iodide; n-butyllithium; ethylenediamine; triethyl phosphite;
In
tetrahydrofuran; hexane; 1,2-dichloro-benzene; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 4 h / Reflux
2.1: triethyl phosphite / 1,2-dichloro-benzene / 5 h / 150 °C
3.1: copper(l) iodide; potassium phosphate; ethylenediamine / toluene / 15 h / Reflux
4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
4.2: 5 h / -78 - 20 °C
With
potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; potassium carbonate; ethylenediamine; triethyl phosphite;
In
tetrahydrofuran; ethanol; hexane; 1,2-dichloro-benzene; toluene;