3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one

Base Information

• Chemical Name: 3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one
• CAS No.: 197777-65-4
• Molecular Formula: C₄₈H₃₈O₁₁P₂
• Molecular Weight: 852.771
• Mol file: 197777-65-4.mol

Synonyms:3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one

Chemical Property of 3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one

There total 1 articles about 3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3',6'-Bis(bis(benzyloxy)phosphanyloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one → 6'-Hydroxy-3'-bis(benzyloxy)phosphoryloxyspiro(isobenzofuran-1(3H),9'-[9H]xanthen)-3-one (197777-67-6) + 3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one (197777-65-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 0.5h; Yields of byproduct given;

DOI:10.1080/00304949709355232

Reference yield: 83.0%

3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one (197777-65-4) → 3',6'-Bis(benzyloxyhydroxyphosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one diammonium salt

Guidance literature:

With ammonium acetate; hydrogen; palladium on activated charcoal; In ethanol; at -5 ℃; for 2h;

DOI:10.1080/00304949709355232

Reference yield:

3',6'-Bis(bis(benzyloxy)phosphoryloxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one (197777-65-4) → 2-(3,6-Bis-phosphonooxy-9H-xanthen-9-yl)-benzoic acid

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 2h;

DOI:10.1080/00304949709355232

Downstream raw materials:

fluorescein diphosphate

3',6'-Bis(phosphonooxy)spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one diammonium salt