N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide

Base Information

• Chemical Name: N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide
• CAS No.: 1459721-85-7
• Molecular Formula: C₃₃H₂₅N₅O
• Molecular Weight: 507.594
• Mol file: 1459721-85-7.mol

Synonyms:N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide

Chemical Property of N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide

There total 1 articles about N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N'-(4-methyphenyl)benzamidine (1859-00-3) + 1,3-diphenylbenzo[e]-[1,2,4]triazin-7(1H)-one (22751-79-7) → N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide (1459721-85-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In toluene; at 100 ℃; for 20h;

DOI:10.1039/c3ob41169a

Reference yield: 22.0%

N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide (1459721-85-7) → N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)benzamide (1403990-53-3) + 8-(4-methylphenyl)-1,3,7-triphenyl-4,8-dihydro-1H-imidazo[4,5-g][1,2,4]benzotriazin-4-yl (1459721-98-2)

Guidance literature:

With acetic acid; at 120 ℃; for 1h;

DOI:10.1039/c3ob41169a

Reference yield:

N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-p-tolylbenzimidamide (1459721-85-7) → N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-phenylbenzimidamide (1459721-84-6)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid / 1 h / 120 °C

2: trichlorophosphate / toluene / 1 h / 20 - 110 °C

3: toluene / 11 h / 20 - 110 °C

With acetic acid; trichlorophosphate; In toluene;

DOI:10.1039/c3ob41169a

upstream raw materials:

N'-(4-methyphenyl)benzamidine

1,3-diphenylbenzo[e]-[1,2,4]triazin-7(1H)-one

Downstream raw materials:

N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-phenylbenzimidamide

N′-n-hexyl-N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e]-[1,2,4]triazin-6-yl)benzimidamide

1,3,7,8-tetraphenyl-4,8-dihydro-1H-imidazo[4,5-g][1,2,4]benzotriazin-4-yl

N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)benzamide