(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

Base Information

Chemical Name:(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol
CAS No.:289909-49-5
Molecular Formula:C₂₀H₃₀O
Molecular Weight:286.458
Hs Code.:

Synonyms:(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

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Technology Process of (S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

There total 2 articles about (S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 75-24-1
trimethylaluminum

: 536-74-3
phenylacetylene

: 80434-59-9,485843-44-5,796865-68-4
(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde

: 289909-49-5
(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

: 289909-74-6
(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

Guidance literature:: trimethylaluminum; With zirconocene dichloride; In dichloromethane;

phenylacetylene; In dichloromethane; at 20 ℃; for 16h;

(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde; In tetrahydrofuran; dichloromethane; at -50 - -10 ℃; for 3h;
DOI:10.1021/ja046084j

Reference yield:

: 66644-32-4
[(1E)-2-iodo-1-methyl-vinyl]-benzene

: 80434-59-9,485843-44-5,796865-68-4
(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde

: 289909-49-5
(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

: 289909-74-6
(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

Guidance literature:: [(1E)-2-iodo-1-methyl-vinyl]-benzene; With vinyliodide; tert.-butyl lithium; In diethyl ether; at -78 - 20 ℃; for 1h;

(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde; In diethyl ether; at -78 ℃; Further stages.;
DOI:10.1021/ol027236n

Reference yield: 85.0%

: 289909-49-5
(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-ol

: 881920-91-8
(E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-phenylbut-2-en-1-one

Guidance literature:: With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 0.583333h;
DOI:10.1021/ol053061g