C₆₀H₇₇N₃O₁₃

Base Information

Chemical Name:C₆₀H₇₇N₃O₁₃
CAS No.:103813-95-2
Molecular Formula:C₆₀H₇₇N₃O₁₃
Molecular Weight:1048.28
Hs Code.:

C<sub>60</sub>H<sub>77</sub>N<sub>3</sub>O<sub>13</sub>

Synonyms:C₆₀H₇₇N₃O₁₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₀H₇₇N₃O₁₃

Chemical Property:

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Technology Process of C₆₀H₇₇N₃O₁₃

There total 18 articles about C₆₀H₇₇N₃O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103813-96-3,103882-19-5,117468-41-4,117556-98-6
5-O-<6-O-benzyl-2,3-O-<6-deoxy-6-ethoxycarbonylamino-2,3,4,7-tetra-O-(p-methylbenzyl)-L-glycero-D-galacto-(R)-heptopyranosylidene>-β-D-talopyranosyl>-1-N,6-O:3-N,4-O-dicarbonyl-1,3-di-N-methyl-2-deoxystreptamine

: 103813-95-2
C₆₀H₇₇N₃O₁₃

Guidance literature:: With barium dihydroxide; In 1,4-dioxane; at 80 ℃;
DOI:10.1016/0008-6215(88)85091-2

Reference yield:

: 6216-32-6
1,3-Bis-N-(benzyloxycarbonyl)-2-desoxystreptamin

: 103813-95-2
C₆₀H₇₇N₃O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1: 52 percent / silver triflate / tetrahydrofuran / 5 h / -78 °C

2: 74 percent / 50 percent NaH / dimethylformamide / 1.) 30 min; 2.) 10 min

3: toluene-p-sulfonic acid / 10 percent Pd/C / methanol / 4 h / 45 °C

4: imidazole / dimethylformamide

5: 30 percent / trimethylsilyl triflate / diethyl ether / 72 h / 3 °C

6: 89 percent / K₂CO₃ / methanol / Ambient temperature

7: pyridinium chlorochromate, molecular sieves 3 A / CH₂Cl₂ / 24 h / Ambient temperature

8: NaBH₄ / ethanol / 1.67 h / 0 °C

9: 0.1 M Ba(OH)2 / dioxane / 80 °C

With 1H-imidazole; barium dihydroxide; sodium tetrahydroborate; trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; palladium on activated charcoal; silver trifluoromethanesulfonate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(88)85091-2

Reference yield:

: 101703-44-0
2,3,4-Tri-O-allyl-6-O-benzyl-α-D-mannopyranosyl chloride

: 103813-95-2
C₆₀H₇₇N₃O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1: 52 percent / silver triflate / tetrahydrofuran / 5 h / -78 °C

2: 74 percent / 50 percent NaH / dimethylformamide / 1.) 30 min; 2.) 10 min

3: toluene-p-sulfonic acid / 10 percent Pd/C / methanol / 4 h / 45 °C

4: imidazole / dimethylformamide

5: 30 percent / trimethylsilyl triflate / diethyl ether / 72 h / 3 °C

6: 89 percent / K₂CO₃ / methanol / Ambient temperature

7: pyridinium chlorochromate, molecular sieves 3 A / CH₂Cl₂ / 24 h / Ambient temperature

8: NaBH₄ / ethanol / 1.67 h / 0 °C

9: 0.1 M Ba(OH)2 / dioxane / 80 °C

With 1H-imidazole; barium dihydroxide; sodium tetrahydroborate; trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; palladium on activated charcoal; silver trifluoromethanesulfonate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(88)85091-2