(1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate

Base Information

Chemical Name:(1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate
CAS No.:1252616-97-9
Molecular Formula:C₂₆H₂₆O₆
Molecular Weight:434.489
Hs Code.:

Synonyms:(1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate

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Chemical Property of (1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate

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Technology Process of (1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate

There total 7 articles about (1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1207286-35-8
C₁₈H₁₈O₃

: 579-75-9
2-Methoxybenzoic acid

: 1252616-97-9
(1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate

Guidance literature:: C₁₈H₁₈O₃; With sodium hydroxide; In water; for 1h; Reflux;

With acetic acid; In water; at 20 ℃; pH=7;

2-Methoxybenzoic acid; Further stages;
DOI:10.1271/bbb.90946

Reference yield:

: 1252617-04-1
2-((1-(hydroxymethyl)cyclohexyl)methyl)naphthalene-1,4-dione

: 1252616-97-9
(1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 1 h / Reflux

2.1: sodium hydroxide / water / 1 h / Reflux

2.2: 20 °C / pH 7

With toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In water; benzene;
DOI:10.1271/bbb.90946

Reference yield:

: 1252617-02-9
C₁₈H₁₈O₂

: 1252616-97-9
(1-((1,4-dihydro-2-hydroxy-1,4-dioxonaphthalen-3-yl)methyl)cyclohexyl)methyl 2-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Cooling with ice

2.1: potassium nitrososulfonate; sodium acetate / methanol; water; N,N-dimethyl-formamide / 5 h / 20 °C

3.1: toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 1 h / Reflux

4.1: sodium hydroxide / water / 1 h / Reflux

4.2: 20 °C / pH 7

With lithium aluminium tetrahydride; potassium nitrososulfonate; sodium acetate; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1271/bbb.90946