methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside

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Chemical Name:methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside
CAS No.:121843-61-6
Molecular Formula:C₂₁H₂₇NO₈
Molecular Weight:421.447
Hs Code.:

Synonyms:methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside

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Chemical Property of methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside

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Technology Process of methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside

There total 7 articles about methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 121843-60-5
methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2,6-dideoxy-6-iodo-α,β-D-glucopyranoside

: 121843-61-6
methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside

Guidance literature:: With pyridine; silver fluoride; Ambient temperature;
DOI:10.1016/S0040-4020(01)97594-5

Reference yield:

: 121843-58-1
methyl 2-acetamido-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-glucopyranoside

: 121843-61-6
methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / Ambient temperature

2: 4-dimethylaminopyridine / 18 h

3: 91 percent / KI / dimethylformamide / 1 h / 100 °C

4: 83 percent / AgF, pyridine / Ambient temperature

With pyridine; dmap; silver fluoride; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)97594-5

Reference yield:

: 121843-56-9
methyl-4,6-O-benzylidene-muramic acid

: 121843-61-6
methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / K₂CO₃ / dimethylformamide / Ambient temperature

2: 73 percent / aq. acetic acid / 1 h / Heating

3: pyridine / Ambient temperature

4: 4-dimethylaminopyridine / 18 h

5: 91 percent / KI / dimethylformamide / 1 h / 100 °C

6: 83 percent / AgF, pyridine / Ambient temperature

With pyridine; dmap; silver fluoride; potassium carbonate; acetic acid; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)97594-5