(3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane

Base Information

Chemical Name:(3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane
CAS No.:1333419-10-5
Molecular Formula:C₁₉H₁₈F₄O₂S
Molecular Weight:386.41
Hs Code.:

Synonyms:(3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane

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Chemical Property of (3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane

Chemical Property:

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Technology Process of (3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane

There total 4 articles about (3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1333418-96-4
2,2,3,3-tetrafluoro-1-(4-methoxyphenyl)-3-(phenylthio)propan-1-ol

: 106-95-6
allyl bromide

: 1333419-10-5
(3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane

Guidance literature:: 2,2,3,3-tetrafluoro-1-(4-methoxyphenyl)-3-(phenylthio)propan-1-ol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

allyl bromide; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201100667

Reference yield:

: 1000293-91-3
trimethyl(1,1,2,2-tetrafluoro-2-(phenylsulfanyl)ethyl)silane

: 1333419-10-5
(3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

With sodium hydride; tetrabutylammonium triphenyldifluorosilicate; In tetrahydrofuran;
DOI:10.1002/ejoc.201100667

Reference yield:

: 108-98-5
thiophenol

: 1333419-10-5
(3-(allyloxy)-1,1,2,2-tetrafluoro-3-(4-methoxyphenyl)propyl)(phenyl)sulfane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide

1.2: -50 - 20 °C

2.1: magnesium / tetrahydrofuran / -78 - 20 °C

3.1: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

With sodium hydride; magnesium; tetrabutylammonium triphenyldifluorosilicate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100667