salicylaldehyde N-(2-nitrobenzoyl)hydrazone

Base Information Edit

Chemical Name:salicylaldehyde N-(2-nitrobenzoyl)hydrazone
CAS No.:316134-13-1
Molecular Formula:C₁₄H₁₁N₃O₄
Molecular Weight:285.259
Hs Code.:
Mol file:316134-13-1.mol

Synonyms:salicylaldehyde N-(2-nitrobenzoyl)hydrazone

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Chemical Property of salicylaldehyde N-(2-nitrobenzoyl)hydrazone Edit

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Technology Process of salicylaldehyde N-(2-nitrobenzoyl)hydrazone

There total 1 articles about salicylaldehyde N-(2-nitrobenzoyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 606-26-8
o-nitrobenzohydrazide

: 90-02-8
salicylaldehyde

: 316134-13-1
salicylaldehyde N-(2-nitrobenzoyl)hydrazone

Guidance literature:: In acetic acid; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/ol801550a

Reference yield: 85.0%

: 316134-13-1
N-[2-NO₂-benzoyl]hydrazone of salicylaldehyde

: 10038-98-9
germaniumtetrachloride

: 412351-56-5
[Ge((C₆H₄)OCHN₂CO(C₆H₄(2-NO₂)))2]

Guidance literature:: In methanol; GeCl4 added to hot satd. soln. of org. ligand (stirring); refluxed (1 h); MeOH partially evapd.; ppt. filtered off; washed with ethanol; dried over CaCl2; elem. anal.;
DOI:10.1023/A:1013755502556