(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide

Base Information

Chemical Name:(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide
CAS No.:338731-19-4
Molecular Formula:C₂₃H₃₀N₂O₆
Molecular Weight:430.501
Hs Code.:

Synonyms:(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide

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Chemical Property of (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide

Chemical Property:

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Technology Process of (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide

There total 3 articles about (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4393-09-3
2,3-dimethoxybenzyl amine

: 338731-27-4
N-2,3-Dimethoxybenzoyl-L-valine

: 338731-19-4
(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 21h;
DOI:10.1055/s-2001-11438

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 338731-19-4
(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxybenztriazole; ethyl(dimethylaminopropyl)carbodiimide / dimethylformamide / 17 h / 0 - 20 °C

1.2: aq. NaOH / dimethylformamide / 14 h

2.1: hydroxybenztriazole; ethyl(dimethylaminopropyl)carbodiimide / dimethylformamide / 21 h / 20 °C

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1055/s-2001-11438

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 338731-19-4
(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-methylbutylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxybenztriazole; ethyl(dimethylaminopropyl)carbodiimide / dimethylformamide / 17 h / 0 - 20 °C

1.2: aq. NaOH / dimethylformamide / 14 h

2.1: hydroxybenztriazole; ethyl(dimethylaminopropyl)carbodiimide / dimethylformamide / 21 h / 20 °C

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1055/s-2001-11438