2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile

Base Information

• Chemical Name: 2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile
• CAS No.: 1358653-97-0
• Molecular Formula: C₂₂H₁₂N₈O₂S
• Molecular Weight: 452.456

Synonyms:2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile

Chemical Property of 2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile

Chemical Property:

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Technology Process of 2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile

There total 3 articles about 2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N,N-dimethyl-4-[(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)ethynyl]aniline (1358653-89-0) + ethenetetracarbonitrile (670-54-2) → 2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile (1358653-97-0)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/ejoc.201101009

Reference yield:

4-bromo-7-nitrobenzo[c][1,2,5]thiadiazole (26460-78-6) → 2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile (1358653-97-0)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: dichloromethane / 1 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; dichloromethane; 1: Sonogashira coupling;

DOI:10.1002/ejoc.201101009

Reference yield:

4-ethynyl-N,N-dimethylaniline (17573-94-3,752235-18-0) → 2-[4-(dimethylamino)phenyl]-3-(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile (1358653-97-0)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: dichloromethane / 1 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; dichloromethane; 1: Sonogashira coupling;

DOI:10.1002/ejoc.201101009

upstream raw materials:

N,N-dimethyl-4-[(7-nitrobenzo[c][1,2,5]thiadiazol-4-yl)ethynyl]aniline

ethenetetracarbonitrile

4-bromo-7-nitrobenzo[c][1,2,5]thiadiazole

4-ethynyl-N,N-dimethylaniline

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