N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine

Base Information

Chemical Name:N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine
CAS No.:55286-16-3
Molecular Formula:C₂₂H₂₇N₃O₂S
Molecular Weight:397.541
Hs Code.:

Synonyms:N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine

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Chemical Property of N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine

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Technology Process of N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine

There total 3 articles about N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.3%

: 2291-58-9
9-benzyl-9-azabicyclo[3.3.1]nonan-3-one

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 55286-16-3
N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine

Guidance literature:: In benzene; Reflux;
DOI:10.1248/cpb.59.1570

Reference yield:

: 111-30-8,29257-65-6,79215-57-9
Glutaraldehyde

: 55286-16-3
N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: water / 20 °C

1.2: 20 °C

2.1: benzene / Reflux

In water; benzene;
DOI:10.1248/cpb.59.1570

Reference yield:

: 100-46-9
benzylamine

: 55286-16-3
N-(9-benzyl-9-aza-bicyclo[3.3.1]non-3-ylidene)-N'-p-toluenesulfonylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / water / 9 h / 20 °C

2: benzene / 24 h / Reflux

With acetic acid; In water; benzene;