2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime

Base Information

Chemical Name:2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime
CAS No.:129508-00-5
Molecular Formula:C₂₇H₂₄N₂O₇
Molecular Weight:488.497
Hs Code.:

Synonyms:2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime

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Chemical Property of 2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime

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Technology Process of 2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime

There total 6 articles about 2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 129507-98-8
2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone

: 129508-00-5
2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime

Guidance literature:: With hydroxylamine hydrochloride; In pyridine; ethanol; for 5h; Heating;
DOI:10.1016/0008-6215(90)84155-N

Reference yield:

: 129507-96-6
Methyl 2-benzamido-3,4-di-O-benzoyl-2,6-dideoxy-α-D-xylo-hex-5-enopyranoside

: 129508-00-5
2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / mercury(II) chloride / acetone; H₂O / 4.5 h / Heating

2: 66 percent / hydroxylamine hydrochloride / pyridine; ethanol / 5 h / Heating

With hydroxylamine hydrochloride; mercury dichloride; In pyridine; ethanol; water; acetone;
DOI:10.1016/0008-6215(90)84155-N

Reference yield:

: 129507-95-5
Methyl 2-benzamido-3,4-di-O-benzoyl-2,6-dideoxy-6-iodo-α-D-glucopyranoside

: 129508-00-5
2L-(2,4,5/3)-4-Benzamido-2,3-dibenzoyloxy-5-hydroxycyclohexanone (E)-oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / silver(I) fluoride / pyridine / 24 h

2: 36 percent / mercury(II) chloride / acetone; H₂O / 4.5 h / Heating

3: 66 percent / hydroxylamine hydrochloride / pyridine; ethanol / 5 h / Heating

With silver(I) fluoride; hydroxylamine hydrochloride; mercury dichloride; In pyridine; ethanol; water; acetone;
DOI:10.1016/0008-6215(90)84155-N