5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide

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Chemical Name:5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide
CAS No.:1338729-25-1
Molecular Formula:C₂₀H₂₅N₃O₄
Molecular Weight:371.436
Hs Code.:

Synonyms:5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide

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Chemical Property of 5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide

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Technology Process of 5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide

There total 2 articles about 5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108352-97-2
5-((4-methoxybenzyl)oxy)-4-oxo-4H-pyran-2-carboxylic acid

: 1338729-25-1
5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / ethanol / 12 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h / 20 °C

With ammonium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 898045-03-9
5-((4-methoxybenzyl)oxy)-4-oxo-4H-pyran-2-carbaldehyde

: 1338729-25-1
5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium chlorite; aminosulfonic acid / water; methanol / 3 h / Cooling with ice

2: ammonium hydroxide / ethanol / 12 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h / 20 °C

With ammonium hydroxide; sodium chlorite; aminosulfonic acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: C₃₉H₄₄IN₅O₁₀S₂

: 1338729-25-1
5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide

: C₅₉H₆₉N₈O₁₃S₂⁽¹⁺⁾

Guidance literature:: C₃₉H₄₄IN₅O₁₀S₂; 5-((4-methoxybenzyl)oxy)-4-oxo-N-(2-(pyrrolidin-1-yl)ethyl)-1,4-dihydropyridine-2-carboxamide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h;

With phosphorus tribromide; In N,N-dimethyl-formamide; at -40 ℃; for 1h;